Abrasive bodies
Abstract
This record has no abstract on file.
Term
Term ended
Expired 31 March 2003, 23.5 years ago.
- Priority
- Filed
- Granted
- Expired
- Today
12 claims: 12 independent, 0 dependent
- 1[Claim(s)] 【特許請求の範囲】 1 (a) 焼結炭化物支持体に接合した研摩材成形体より成る複合研摩材成形体を提供する工程;(b) ニツケル、銅、コバルト、鉄又はこれらの金属の1種もしくはそれ以上を含有する合金の層を、金属含有基板表面に析出させ、該金属層に横圧力を加え、該金属層の温度をその融点以下の温度に上げ、該圧力及び温度を該金属層が該基板に接合できるようにさせるのに十分な時間にわたつて維持する工程;(c) 該金属層の露出表面を研摩する工程;(d) 該支持体及び基板を共に、該金属層が該支持体表面に接触するような状態にさせる工程;(e) 該支持体及び基板に横圧力を加えることにより該支持体及び基板を共に圧迫する工程;(f) 該金属層の温度を、その融点以下の650 ゚~750°Cの範囲の温度に上げる工程;及び(g) 該支持体と基板との間に拡散接合が生ずるのに十分な時間にわたつて上記圧力及び温度を維持しつつ、前記工程(f)及び(g)を不活性雰囲気下に行う工程;を含む、研摩材成形体と、該研摩材成形体に接合する焼結炭化物支持体と、ニツケル、銅、コバルト、鉄またはこれらの金属の1種もしくはそれ以上を含有する合金の層を通して該支持体に接合する金属含基板とより成る、研摩本体を製造する方法。 A method characterized by comprising the following of manufacturing a polish main part, 1 (A) Process;(B) of Providing a Compound Polish Material Fabrication Object Which Comprises a Polish Material Fabrication Object Joined to a Sintering Carbide Base Material Nickel, A layer of an alloy containing more than one sort or it of copper, cobalt, iron, or such metal, A metal content substrate face is deposited, horizontal force power is applied to the metal layer, and temperature of the metal layer is raised to temperature below the melting point, Process;(c) of carrying out cotton intermediary maintenance at time sufficient although the metal layer can make it enabling it to join the pressure and temperature to the substrate Process;(d) of grinding the exposure surface of the metal layer It is about the both base materials and substrates, Process;changed into the state where the metal layer contacts the support surface (e) Process;(f) of pressing the both base materials and substrates by applying horizontal force power to the base material and substrate Temperature of the metal layer, Process;raised to temperature of the range of 650 *~750-degreeC below the melting point, and (g) A polish material fabrication object which includes process;of performing said process (f) and (g) under an inactive atmosphere maintaining the cotton intermediary above-mentioned pressure and temperature at sufficient time for diffused junction to arise between the base material and substrate A sintering carbide base material joined to the polish material fabrication object, Metal Containing substrate joined to the base material through a layer of an alloy containing more than one sort or it of nickel, copper, cobalt, iron, or such metal.
- 22 Horizontal Force Power Applied to a Base Material and a Substrate is 40~300Ns/Mm.2A method of an application for patent which is Range given in the 1st paragraph of a range. 2 支持体及び基板に加える横圧力が40~300N/mm2の範囲である特許請求の範囲第1項記載の方法。
- 33 A method given in the 1st paragraph of a range or the 2nd paragraph of an application for patent which carries out cotton intermediary maintenance of pressure and the temperature in 5~300 minutes. 3 圧力及び温度を5~300分間にわたつて維持する特許請求の範囲第1項又は第2項に記載の方法。
- 44 A method of an application for patent which carries out cotton intermediary maintenance of pressure and the temperature in 5~35 minutes given in the 3rd paragraph of a range. 4 圧力及び温度を5~35分間にわたつて維持する特許請求の範囲第3項記載の方法。
- 55 工程(d)の状態になつた後の基板及び支持体を、内部に形成された空洞を有する包囲物体と、該空洞内に置かれ該包囲物体の熱膨張係数よりも大きな熱膨張係数を有する膨張物体とより成る組立部品の空洞内に配置し、次いで該組立部品の温度を工程(f)の所望温度に上げ、それにより該膨張物体を膨張させて工程(e)の所望の横圧力を該支持体及び基板に加える特許請求の範囲第1項~第4項のうち任意の1項に記載の方法。 It is a method given in the 1st arbitrary paragraph among the 1st paragraph [ of a range ]~4th paragraph of an application for patent characterized by comprising the following which arranges in a cave of assembling parts, subsequently to request temperature of a process (f), raises temperature of the assembling parts, expands the expansion object by that cause, and applies horizontal force power of a request of a process (e) to the base material and substrate. 5 Envelopment Object Which Has Cave Formed in Inside in Substrate and Base Material after Noodle at State of Process (D), An expansion object which is placed in the cave and has a bigger thermal expansion coefficient than a thermal expansion coefficient of the envelopment object.
- 66 A method of an application for patent which raises temperature of assembling parts by putting the assembling parts in a furnace given in the 5th paragraph of a range. 6 組立部品の温度を該組立部品を炉中に入れることにより上げる特許請求の範囲第5項記載の方法。
- 77 The 5th paragraph of a range of an application for patent or a method given in the 6th paragraph of being a product made from ceramics to which an envelopment object is based on a product made from sintering carbide, silicon nitride, or zirconia. 7 包囲物体が焼結炭化物製又は窒化ケイ素もしくはジルコニアをベースとするセラミツク製である特許請求の範囲第5項又は第6項記載の方法。
- 88 An expansion object is a method given in the 1st arbitrary paragraph among the 5th paragraph [ of a range ]~7th paragraph of an application for patent which is a product made from nimonic. 8 膨張物体がニモニツク製である特許請求の範囲第5項~第7項のうち任意の1項に記載の方法。
- 99 Pressure Applied to a Metal Layer is 1~200Ns/Mm.2A method of an application for patent which is Range given in the 1st paragraph of a range. 9 金属層に加える圧力が1~200N/mm2の範囲である特許請求の範囲第1項記載の方法。
- 1010 The 1st paragraph of a range of an application for patent or a method given in the 9th paragraph temperature from which a metal layer is raised is the range of 700~1100 degreeC. 10 金属層の上げられる温度が700~1100°Cの範囲である特許請求の範囲第1項又は第9項記載の方法。
- 1111 A method given in the 1st paragraph of a range of an application for patent which carries out cotton intermediary maintenance of pressure and temperature which are applied to a metal layer in 5~300 minutes, the 9th paragraph, or the 10th paragraph. 11 金属層に加える圧力及び温度を5~300分間にわたつて維持する特許請求の範囲第1項、第9項又は10項に記載の方法。
- 1212 It is a method given in the 1st arbitrary paragraph among the 1st paragraph of a range of an application for patent which carries out cotton intermediary maintenance of pressure and temperature which are applied to a metal layer in 5~30 minutes, or the 9th paragraph~11th paragraph. 12 金属層に加える圧力及び温度を5~30分間にわたつて維持する特許請求の範囲第1項又は第9項~第11項のうち任意の1項に記載の方法。
Independent claims12
4 paragraphs, as filed
[Detailed Description of the Invention]
The background of an invention The present invention relates to a polish main part. It buries for [ which is marketed now ] drill crown (drilcrown), and is one sort of a golden (insert) element or a cutting element, The diamond fabrication object (compact) joined to the metallic bond (sintering) carbide (cementedcarbide) base material is comprised, and the base material is joined to the one by one more big metallic bond carbide board with wax here. The wax has the melting point more than 700 degreeC, and under the severe condition which exists generally [ while using the drill crown ], the good junction between the substrate and base material is attained certainly, and it maintains it. While burying and soldering the base material to a substrate during golden manufacture, it must warn to secure that powdering of a diamond fabrication object layer does not arise. this -- under the soldering -- a diamond fabrication object -- heat -- it can attain being useless (heat sink) and by making it contact. The abstract of an invention Present invention: a polish material fabrication object; The sintering carbide (hard metal) base material joined to b this polish material fabrication object; it reaches. The polish main part which comprises the metal content board joined to the base material through the joining layer which comprises the alloy containing more than one sort or it of c nickel, copper, cobalt, iron, or these metal is provided. The layer of the alloy which contains more than one sort or it of nickel, copper, cobalt, iron, or these metal if it carries out from another viewpoint of the present invention, The manufacturing method of the above-mentioned polish main part which includes the process inserted between the sintering carbide support surfaces which the forming object has joined to the substrate face, and the process of carrying out diffused junction of the base material to the substrate at the temperature below the melting point of the insertion layer via the insertion layer is provided. The detailed statement of an invention A polish material fabrication object comprises the multi-crystal collection lump of the nature polish material particles of superhard which are common knowledge and were combined with this industry in the shape of a hard aggregate. Such a forming object generally has the second phase that always contains the catalyst [ especially as opposed to the nature polish material particles of superhard ] of the forming object, or a solvent, or a junction phase. It is publicly known now and the nature polish material of superhard currently used for the forming object is a diamond and Legal crystal (cubic) boron nitride. these arbitrary industries [ like sintering titanium carbide, sintering tantalum carbide, sintering tungsten carbide, or those mixtures ] in which the sintering carbide base material is -- it may be publicly known. The metal phase to such sintering carbide is generally Nitsugawa, cobalt, or iron which exists in the quantity from 3 % of the weight to 35 % of the weight. It can join to the carbide base material directly, or can join the polish material fabrication object to the carbide base material through a joining layer. The polish material fabrication object joined to the sintering carbide base material is known also as "a compound polish material fabrication object (composite abrasive compact)." The example of a polish material fabrication object or a compound polish material fabrication object can be found out on British patent No. 1489130, U.S. Pat. No. 3745623, and 3743489 each specifications. These indications are included in this specification as reference. The substrate is generally larger than the sum total mass and sum total capacity of the polish material fabrication object and the carbide base material in mass and capacity. Although the substrate is generally sintering carbide (hard metal), it can also be steel like hardened steel. The joining layer between the base material and substrate generally has the thickness up to 220 microns. It is high, namely, the Takeshi strength which junction between the base material and substrate does not carry out is 140Ns/mm.<sup>2</sup>Or it is I and It was that it can be more than it. The polish main part of the present invention has a use as a component to a polishing tool. the especially polish main part receives A bit or crown of a drill -- it buries and has a use as gold, i.e., a cutting element. The example of such a cutting element is shown in Drawing 1 of a drawing. The cutting element which comprises disc-like polish material fabrication object 10 joined to sintering carbide base material 12 in this figure is shown. The carbide base material 12 is arranged in hollow 14 in substrate 16 prolonged for a long time. Junction to substrate 16 of the carbide base material 12 is performed through joint layer 18 of the form mentioned above. The polish main part of the present invention is the British patent No. 1489130 first, Although it writes in U.S. Pat. No. 3745623 and 3743489 each specification, generally by manufacturing the compound polish material fabrication object which comprises the polish material fabrication object joined to the sintering carbide base material by the method publicly known in this industry [ like ], it is obtained. Subsequently, diffused junction art is applied and the compound polish material fabrication object is joined to a substrate through the above defined joining layer. Although diffused junction is publicly known in this industry and it is a method which junction of metal versus metal is made to produce, in this case, a metal atom carries out horizontal OFF intermediary movement of the bonded surface, and forms continuation crystalline particles. This method is solid phase synthesis and metal has not reached that melting point. As for diffused junction, it is I and It was to produce the junction which has the outstanding intensity between the base material and substrate, when it is under the condition that the damage over the polish material particles of a polish material fabrication object is avoided on substance. If it puts in another way, in the case of a diamond fabrication object, the forming object does not contain black lead on substance, and, in the case of a cubic boron nitride fabrication object, does not contain hexagonal boron nitride on substance. desirable -- this method -- the following process, i.e., : (a) Process of providing the compound polish material fabrication object which comprises the polish material fabrication object joined to the sintering carbide (hard metal) base material; (b) The layer of the alloy containing more than one sort or it of nickel, copper, cobalt, iron, or such metal, Process of carrying out cotton intermediary maintenance at time sufficient although a metal content substrate face is deposited, horizontal force power is applied to the metal layer, the temperature of the metal layer is raised to the temperature below the melting point and the metal layer can make it enabling it to join the pressure and temperature to the substrate; (c) Process of grinding the exposure surface of the metal layer; (d) Process at which the both base materials and substrates are made to change into the state where the metal layer contacts the support surface; (e) Process of pressing the both base materials and substrates by applying horizontal force power to the base material and substrate; (f) process; of raising the temperature of the metal layer to the temperature of the range of 650 *~750-degreeC below the melting point -- and (g) Include process; of performing the above-mentioned process (f) and (g) under an inactive atmosphere, maintaining the cotton intermediary above-mentioned pressure and temperature at sufficient time for diffused junction to arise between the base material and substrate. The pressure applied while carrying out diffused junction of the base material to a substrate is generally 40~300Ns/mm.<sup>2</sup>It comes out, and it is and temperature is a grade of 650~750 degreeC typically. Diffused junction is 10.<sup>-4</sup>The damage which arises to the polish material particles of a line intermediary and the polish material fabrication object under Thor, a still better vacuum, or other inactive atmosphere like inactive gas is minimized. the pressure and temperature -- 5~ -- cotton intermediary maintenance can be carried out typically in 5~35 minutes, and good junction can be ensured for 300 minutes. In the present invention method, the horizontal force power can be applied to this industry that uses an oil pressure cylinder press, for example by a publicly known method. In one special method of applying desired horizontal force power to the base material and substrate, the difference of the thermal expansion coefficient between an external envelopment object and an internal expansion object is used. The base material and substrate after changing the both methods into the state of the above-mentioned process (c), It is arranged in the envelopment object which has the cave formed in the inside, and the cave, and puts in in the cave of the assembling parts which comprise the expansion object which has a bigger thermal expansion coefficient than the envelopment object, Subsequently, it includes raising the temperature of the assembling parts to the request temperature of the above-mentioned process (e), expanding the expansion object by that cause, and applying the horizontal force power of a request of the above-mentioned process (d) to the base material and substrate. Typically, the temperature of the assembling parts is To raise the temperature by putting the assembling parts in a furnace. The envelopment object can be a product made from ceramics based on the product made from sintering carbide, silicon nitride, or zirconia. The expansion object is the metal or the product made from an alloy which has a typically high thermal expansion coefficient. the alloy of the example of a suitable alloy based on nickel is nimonic (Nimonic) -- it is . The cavernous side in contact with the expansion object can be made to be able to incline, and can be adjusted in the slope of the expansion object. Or instead, the expansion object has two contact portions, and the contact surface may incline and consistent. When the expansion object reacts to the element joined under application temperature conditions in harmful, an inactive filling thing suitable between the expansion object and the element joined can be supplied. This pressurizing method is applied [ as opposed to / especially / joining a compound polish material fabrication object to a tool pedicel (that is, a tool pedicel is a substrate) ]. Drawings 2 and 3 of a drawing illustrate the embodiment in the above-mentioned viewpoint of the present invention. In these drawings, assembling parts 20 which comprise envelopment object 22 which has A groove or cave 24 formed into it by the product made from sintering carbide are shown. Envelopment object 22 is attached to hollow 26 in steel supporting boards 28. He would like to be opposed to cave 24, rust 30 and 32 is arranged, and these have a Along contact slope in straight line 34. These wedges are the products made from alloy nimonic. In the cave, packing element 36 in contact with surface 38 of wedge 32 is also arranged. Tool pedicel 42 is arranged between packing element 36 and surface 40 of the envelopment object, and the tool pedicel has compound polish material fabrication object 44 and the junction relations which comprise polish material fabrication object 46 joined to sintering carbide base material 48. Between tool pedicel 42 and base material 48, suitable thin metal layer 50 to produce diffused junction between the tool pedicel and base material is arranged. In order to make the effective diffused junction between a tool pedicel and a base material attain, the whole assembling parts are put in the furnace at a suitable temperature. The temperature must be the temperature which produces diffused junction. At this temperature, wedges 30 and 32 made from nimonic expand at a speed quicker than envelopment object 22. It has the effect that this makes junction pressure power act on tool pedicel 42 and base material 48. It is it is important and desirable to grind the exposure surface of a metal layer, in order to secure making the surface as flat as possible. Polish can be performed by using a diamond polishing tool. The surface of the base material to which a substrate is joined should also be made as flat as again possible. Especially the metal layer joined to a substrate face is distorted during polish, and has a twisted tendency. In order to minimize this tendency, a metal layer is deposited to a substrate face and horizontal force power is applied to the metal layer, It is I and It was that it is preferred to raise the temperature of the metal layer to the temperature below the melting point, and to, carry out cotton intermediary maintenance of the pressure and temperature subsequently to the substrate at time sufficient although the metal layer can join. Typically, the pressure applied to the metal layer is 1~200Ns/mm.<sup>2</sup>It is Range and the temperature from which the metal layer is raised is 700degreeC~1100degreeC. the conditions of such temperature and pressure -- 5~ -- cotton intermediary maintenance can be carried out typically in 5~30 minutes for 300 minutes. The metal can be deposited to a substrate face by a method publicly known in this industry like making the surface which contacted electroplating, unelectrolyzed plating, vapor deposition, sputtering, or metallic foil to the substrate, and has arranged it or on which the substrate carried out metallic coating of the metallic foil contact, and arranging. The horizontal force power can be applied to a metal layer by a method publicly known in this industry. the thin metallic coating of the metal used for coating point Stand up to contact the carbide base material and metallic coating surface of a substrate, and coating with the substrate face the support surface which should be joined, and an identical or similar metal -- Apply -- things are made. Such a metal layer can deposit electroplating, unelectrolyzed plating, vacuum deposition, and this industry like sputtering by a publicly known method on the surface of the base material. The following example further explains the present invention. Example 1 The disk of annealing nickel was deposited on the surface of stub (stub) made from tungsten carbide which carried out cobalt combination. It is 100Ns/mm to this nickel covering surface.<sup>2</sup>Pressure was applied and temperature was raised to 830 degreeC. It was which maintains these conditions for 20 minutes. Subsequently, the exposure surface of the nickel layer was ground with the diamond polishing tool. The thickness of nickel covering is 120 microns and is Oh. The compound polish material fabrication object of the disk shape which comprises the diamond fabrication object joined to the base material of the tungsten carbide which carried out cobalt combination was manufactured by the method of the statement on the British patent No. 1489130 specifications. Subsequently, the compound polish material fabrication object was joined to the stub by contacting the back of the base material to the nickel layer on the stub first. 290Ns/mm horizontal force power<sup>2</sup>In addition to the With compound polish material fabrication object and the stub, both these both were pressed and the temperature of the border plane, i.e., a nickel layer, was raised to 725 degreeC. This processing is 10.<sup>-4</sup>In Thor's vacuum, it is I got it. It was which maintains these conditions for 30 minutes. The junction outstanding between the carbide base material and carbide stub with this diffused junction art was attained. The Takeshi strength which the junction does not carry out is measured, and it is 390Ns/mm.<sup>2</sup>It is I and It was that it is a of grade. The thickness of the joining layer between the base material and stub is a 120-micron grade, and is Oh. Example 2 Conditions of this intermediary following [ join / to a compound polish material fabrication object / the stub which carried out nickel covering ]: Applied pressure 270Ns/mm<sup>2</sup>Heating temperature 730degreeC Maintenance conditions 300-minute nickel covering 200 microns It is Ivy although the procedure given in the above-mentioned Example 1 was used except for the adopted point. The Takeshi strength which junction between a carbide base material and a stub does not carry out is 400Ns/mm.<sup>2</sup>It is I and It was that it is above.
[Brief Description of the Drawings]
Drawing 1 is a side view of the embodiment of the polish main part of the present invention. Drawing 2 is a side sectional view of the assembling parts for using it for the present invention method. Drawing 3 is a partial section perspective diagram of the assembling parts of above-mentioned Drawing 2.
Every citation, both ways
| Document | Relation | Office | Cited during |
|---|---|---|---|
| WO2020262608A1 | Cited by | World Intellectual Property Organization (WIPO) | International search |
17 members in 6 offices
Priority claims4
| Document | Office | Kind | Date |
|---|---|---|---|
| 8209409 | United Kingdom | A | |
| 8209409 | – | – | – |
| 8302620 | – | – | – |
| GB19820009409 | – | – | – |
Members17
| Document | Office | Kind | |
|---|---|---|---|
| GB8302620D0 | United Kingdom | D0 | |
| EP0090657A2 | European Patent Office (EPO) | A2 | |
| EP0090658A2 | European Patent Office (EPO) | A2 | |
| ZA831948B | South Africa | B | |
| ZA831949B | South Africa | B | |
| JPS58211861A | Japan | A | |
| JPS58217270A | Japan | A | |
| EP0090657A3 | European Patent Office (EPO) | A3 | |
| EP0090658A3 | European Patent Office (EPO) | A3 | |
| US4496372A | United States of America | A | |
| US4505721A | United States of America | A | |
| EP0090657B1 | European Patent Office (EPO) | B1 | |
| DE3368886D1 | Germany | D1 | |
| EP0090658B1 | European Patent Office (EPO) | B1 | |
| DE3372267D1 | Germany | D1 | |
| JPH034336B2This record | Japan | B2 | |
| JPH0356868B2 | Japan | B2 |
Numbers
- Publication, DOCDB
- H034336
- Publication, EPODOC
- JPH034336B
- Application
- 58056812
- Application, DOCDB
- 5681283
- Application, EPODOC
- JP19830056812
Classification
- IPC, 7
- B23B27 14
- B23B27 00
- B23P15 28
- B24D
- B24D3 10
- B25D17 02
- B32B15 01