Method for inspecting leakage of sealed container.

BACKGROUND OF THE INVENTION

[Field of the Invention]

0001This invention relates to a method for inspecting leakage of a sealed container, and more particularly to an inspection method effectively used for inspecting a leaking place such as a pin hole, a crack, etc. of a sealed container containing foods, pharmaceuticals, chemical industrial products or the like.

[Description of the Prior Art]

0002In a food industry, there are generally used containers of a type in that containers are sealed after foods are filled therein and then sterilized by heating, or of a type in that containers are sealed after foods are filled therein under a bacteria-free condition. In these containers, if there occurs a poor sealing, a pin hole or the like, air tends to flow into the containers through the pin hole, etc. from outside and a bacterial contamination is taken place. As a result, foods as the contents of the containers are oxidized, changed in quality, or corrupted. In some cases, it turns out to be a significant problem endangering a human life.

0003Therefore, in a food industry or a container manufactur­ing industry, many attempts have been made in order to develop an improved art for sealing with a hope to provide a perfect sealing of a container, an improved art for inspec­tion for inspecting the sealing of a container, and a related instrument, device, apparatus, etc. Representative examples thereof are as follows. <ul id="ul0001" list-style="none"><li>(1) One of the representative methods for inspecting leakage of a food can using a metallic can is known as a beat inspecting method. According to this method, an objective container is beaten with a metallic bar and the sealing is inspected by checking with the beating sound. However, this beat inspecting method is inapplicable to a compound con­tainer of plastic material with aluminum foils laminated thereon.</li><li>(2) As another example, there is a method for inspecting the sealing of a container, in which an objective container is formed with a hole, the peripheral area of the opening portion of the hole is sealed with a rubber material or the like and then, the container is sunk into water, and there­after, air is sent into the hole in order to raise the inter­nal pressure of the container and finally, generation of an air bubble from the container is checked. This method, however, has the shortcoming in that breakage of the objec­tive container is unavoidable.</li><li>(3) In a retort food, there is employed a method in that a bag-shaped container formed of a laminated film of aluminum foil and plastic, or a plastic film vapor deposited with aluminum is used, and air is removed from the container after the container is filled with foods, or otherwise an inert gas such as a nitrogen gas or a carbon dioxide gas or a mixture of a nitrogen gas and a carbon dioxide gas is charged into the container after air is removed from the container, and then the container is sealed. As a seal inspecting method of a retort food, there is employed a method in that an objective container containing food therein is kept for two to three weeks at a normal tem­perature of 25°C to 40°C and any expansion of the objective container caused by bacterial contamination or any oozing-out of a liquid content filled in the container, which tends to occur when imperfect sealing, pin-hole, etc. are taken place, is inspected by eye. However, any of the above-mentioned methods has the problems in that many days are required for carrying out this inspection and a large stock of the objec­tive containers is required.</li><li>(4) As still another method for inspecting any leakage, there is known a method in that a container having a con­firmed perfect sealing and an objective container are accom­modated in two vacuum chambers which are perfectly sealed and separated, and thereafter, any change of an internal pressure of the vacuum chambers, which tends to occur when an imper­fect sealing of the objective container, a pin-hole, etc. are detected, by using a so-called pressure sensor under a predetermined reduced pressure. However, this method again has the shortcoming in that when moisture is attached to the external part of the container, a correct leakage inspection is difficult to obtain because the internal pressure of the chambers is also readily changed owing to evaporation of the moisture when the pressure is reduced.</li><li>(5) There is also a method for determining any leakage in that a vacuum chamber is filled with water, and after the objective container is dipped in the water, the internal pressure of the chamber is reduced, and finally, any bubble or any oozing-out of the content of the objective container is inspected. However, this method has the problem that an additional procedure for drying the container is required after inspection because the objective container is wet with the water.</li></ul>

0004As described above, the conventional inspecting methods have the various problems in that the objective container is limited, a correct inspection is difficult to obtain, the manner for carrying out the method is complicated and a long period of time is required for carrying out the method, and so on.

SUMMARY OF THE INVENTION

0005An object of the present invention is to provide a method for inspecting leakage of a sealed container which is applicable to any desirable sealed container irrespective of its forming material, shape, content, etc., and in which ob­jective containers can be individually, easily, rapidly and correctly inspected through a simple procedure.

0006The above object can be achieved by providing a method for inspecting leakage of a sealed container comprising changing an internal pressure of a vacuum chamber provided therein with an eddy-current displacement sensor to a predetermined degree of vacuum from a normal pressure after putting a sealed container having a conductive material at least at a portion to be inspected in the chamber; detecting an amount of expansion of said sealed container at said degree of vacuum in time sequence by said eddy-current dis­placement sensor; and determining whether any change occurs or not in the amount of expansion after a time when the detected amount of expansion amount shows the maximum value, thereby to find out any pin hole formed in said sealed con­tainer.

0007Not only an eddy-current displacement sensor, any kinds of sensors that can measure very small displacement are use­ful in this method. An infrared sensor, a supersonic wave sensor, a laser beam sensor, an optical sensor, etc. are as useful as an eddy-current displacement sensor in this leakage detecting method.

0008According to the method for inspecting leakage of a sealed container of the present invention, this method is ap­plicable to any desirable sealed container irrespective of its forming material, shape, content, etc., and any pin hole formed in the objective containers can be individually, easily, rapidly and correctly inspected.

[Function]

0009In the method of the present invention, as described above, in the case that an internal pressure of a vacuum chamber is maintained in a predetermined degree of vacuum where the sealed container shows the maximum value of expan­sion, the maximum amount of expansion can be maintained when the container has no pin hole, etc., and on the contrary, when the container has a pin hole, etc., the amount of expan­sion is reduced from the maximum value in time sequence. As this aging change can correctly be detected by an eddy-­current displacement sensor, there can correctly be inspected whether a sealed container has a pin hole or not.

0010The above and other objects and features of the present invention will be apparent from the following detailed description and appended claim when taken in conjunction with the accompanying drawings.

BRIEF DESCRIPTION OF THE DRAWINGS

0011<ul id="ul0002" list-style="none"><li>Fig. 1 is a schematic view of a leak inspecting ap­ paratus which is employed for carrying out a method of the present invention;</li><li>Fig. 2 is a graph showing aging change of the amount of expansion of a sealed container; and</li><li>Fig. 3 is a schematic front view for explaining the aging change of the amount of expansion of the sealed con­tainer.</li></ul>

DETAILED DESCRIPTION OF THE INVENTION

0012One preferred mode of the present invention will now be described.

0013First, one example of a leak inspecting apparatus for a sealed container, which is employed in this mode for carrying the method of the present invention will be described with reference to the accompanying drawings.

0014Fig. 1 is a schematic view of the leak inspecting ap­paratus. Reference numeral 1 shown in section in the figure generally denotes a vacuum chamber for accommodating therein a sealed container 2 as an object to be inspected. The chamber 1 includes a chamber section 1a and a lid member 1b. Interposition between the chamber section 1a and the lid mem­ber 1b is an O-ring 3 adapted to keep the chamber 1 air tight.

0015And, the chamber section 1a is connected to a vacuum pump 6 through a piping 4 and a buffer vacuum tank 6. The piping 4 is provided with a pressure sensor 7 for detecting an internal pressure of the chamber 1 and a solenoid valve 8 for opening and closing the piping 4.

0016Further, the lid member 1b is provided with an eddy-­current displacement sensor 9 secured to a central position of an upper part thereof through a support member 9a.

0017Furthermore, the pressure sensor 7, the solenoid valve 8 and the eddy current displacement sensor 9 are electrically connected with a control device 10 respectively. By virtue of the foregoing arrangement, the interior of the chamber 1 can correctly be maintained in a desired degree of vacuum, and at the same time an output voltage of the eddy-current dis­placement sensor 9 is detected so that there can be deter­mined whether there is a cause of leakage such as a pin hole, etc. in the container 2. The control device 10 is provided with a first lamp 10a which is lighted up when the amount of leakage is large and a second lamp 10b which is lighted up when the amount of leakage is small.

0018Also, the vacuum tank 5 is provided with a pressure gauge 11 and a pressure sensor 12. The pressure sensor 12 as well as the vacuum pump 6 are electrically connected to a control switch 13 so that the interior of the vacuum tank 5 can always be maintained in a desired degree of vacuum.

0019In the case that the method of the present invention is carried out by using the above-mentioned apparatus, first, as shown in Fig. 1, the sealed container 2 is placed in a predetermined position within the vacuum chamber 1. There­after, the solenoid valve 8 is activated so that the degree of vacuum in the vacuum chamber 1 is changed from a normal pressure to a predetermined degree of vacuum in order to ex­pand the container 2. And the interior of the chamber 1 is maintained in the aforementioned predetermined degree of vacuum and the amount of expansion (amount of an increase in height) of the sealed container is detected by the eddy-­current displacement sensor 9 in time sequence in the afore­mentioned degree of vacuum.

0020When the aging change of the amount of expansion after a time point where the detected amount of expansion (output voltage) shows the maximum value is chased, the maximum amount of expansion (maximum output voltage) is maintained provided that there are no pin hole, etc. in the container. On the contrary, if there is a pin hole, etc., the amount of expansion (output voltage) is reduced in time sequence. Therefore, by detecting the aging change, there can be deter­mined whether there are a pin hole, etc. in the sealed con­tainer 2.

0021Fig. 2 is a graph which concretely shows the aging change of the amount of expansion in order to enhance an easy understanding.

0022In Fig. 2, the horizontal axis shows time (sec.), the left-hand vertical axis shows degree of vacuum (mmHg) in a chamber and the right-hand vertical axis shows an output voltage of an eddy-current displacement sensor corresponding to the degree of expansion of a container.

0023In the figure, A denotes an orbit of the aging change of an internal pressure of the chamber, B and C denote orbits of the aging change of an amount of expansion of the container accommodated in the chamber which is changed in pressure ac­cording to the orbit of A. B represents a case where there are no pin hole, etc., whereas C represents a case where there are a pin hole, etc.

0024An air removal step is started at time t₁, a predeter­mined degree of vacuum is reached at time t₃, said degree of vacuum is maintained until time t₄, and thereafter, it is leaked into atmosphere to completely return to a normal pres­sure at time t₅ (orbit A). This degree of vacuum is properly selected in accordance with the kind of objective containers.

0025The amount of expansion of a container having no pin hole, etc. at the time zone from t₁ to t₅ will be described with reference to the orbit B showing the change of the amount of expansion. The amount of expansion is increased as the air removal is progressed in the chamber, it reaches the maximum value P at time t₃ and the amount of expansion is maintained in that level until time t₄.

0026On the other hand, the amount of expansion of a con­tainer having a pin hole, etc. (hereinafter sometimes referred to as the "leak can") in the same time zone as above likewise shows the maximum value P′ at time t₃ as shown in the orbit C. In this case, however, the amount of expansion is gradually reduced in time sequence until it reaches time t₄. The degree of gradual reduction (inclination) is larger as a cause for leakage such as a pin hole, etc. are larger.

0027Before the degree of pressure reduction in the chamber 1 reaches a predetermined pressure level, if, for example, the detection of the amount of expansion is started at a time point of time t₂, the maximum value P or P′ of the amount of expansion can easily be specified. Also, even in a case where a container (hereinafter referred to as the "large leak can") has so large cause for leakage as that the amount of expansion of the container at preestablished time t₂ for starting the detection is unable to reach a measuring level V and the value of expansion is hardly changed during a period of time for measurement as in the orbit D, the container can be detected as the leak can.

0028In an apparatus as shown in Fig. 1, in the case that the container has a pin hole, etc., the lamp is automatically lighted up. Moreover, as the first and second lamps 10a and 10b are selectively lighted up by determining whether the size of the pin hole, etc. is large or small, It can im­ mediately detected whether there are a pin hole, etc. in the container and whether the size of the pin hole, etc. is large or small.

0029As described in detail in the foregoing, according to a method of the present invention, there can easily be deter­mined whether there are a pin hole, etc. in a container by chasing the aging change of the amount of expansion of a con­tainer under a predetermined degree of reduced pressure.

0030Also, in a method of the present invention, as various containers can be individually detected, a standard object or a standard value, etc. are not required. Accordingly, there can be obtained an absolute inspection irrespective of kind of a container, for example, an accommodating substance, material, shape, size, etc. Figs. 3(a) through 3(c) con­cretely shows this (in the illustrated examples, containers i and iii have no pin hole, etc. while a container ii is a leak can. Similarly, a container iv is a large leak can.).

0031That is, as described in the foregoing, according to a method of the present invention, as objective containers can individually be detected, even in a case as shown in Fig. 3(a) where containers are of the same kind (the heights thereof are all A under a normal pressure) but they have in­dividual differences, the heights (amount of expansion) after expansion can be detected as inherent values a and c (a # c) to the respective containers as shown by the containers i and iii (Fig. 3(b)). As such values can be maintained in time sequence (Fig. 3(c)), it can be determined that the con­tainers i and iii have no pin hole, etc. From a fact that the heights of the container ii after expansion exceeds a preestablished measuring level and the height b is changed to b′ in time sequence, it can be determined that the container has a pin hole, etc. In this way, there can be determined whether there are a pin hole, etc. even for same kinds of containers irrespective of individual differences thereof. Further, in a case of a container having the height not reaching the preestablished measuring level V, it can be detected as a large leak can without largely showing the change of the amount of expansion from d to d′ at a time when measuring.

0032The apparatus of Fig. 1 will be described in more detail. As material forming the lid member 1b constituting the chamber 1, there can be selected from various materials such as plastic, ceramic, etc. as long as they do not shelter a magnetic field and they can maintain a vacuum.

0033Also, as an eddy-current displacement sensor which is applicable to the above-mentioned apparatus, there can be listed, for example, AH-422 of Kabushiki Kaisha Keyence. At that time, there can be used AS-440-10 of the same company as a controller.

0034Also, as a sealed container to which a method of the present invention is applicable, all kinds of containers (including bag-like containers) can be of its object ir­respective of contents, material, shape, size, etc. However, in a case that the lid member is solely made of a nonconductive substance such as plastic, etc., it is neces­sary to provide a conductive material such as aluminium foil, etc. onto at least a part to be inspected (for example, a part of the lid) corresponding to a detecting surface of an eddy-current displacement sensor.

0035Also, the degree of vacuum required during the inspec­tion is suitably changed depending on an objective container. The period of time required is also changed depending on the inspection condition. As one example, when the lid is formed of plastic and the container is laminated with aluminum foil at its inner surface, a required period of time was 20 to 30 seconds when the bore of a pin hole was 15µ and a few seconds when the bore was 70µ all under the condition that the degree of vacuum (degree of reduced pressure) was 400 to 500mmHg at an inspecting time. Also, as a degree of vacuum applicable to an ordinary metallic can, there can be listed 500 to 600mmHg as a preferable range.

0036Although a method of the present invention has been described in a mode for carrying out the method, the present invention is not limited to the above-mentioned mode for car­rying out the method.

0037For example, a leak inspecting device to be employed may, of course, be of a type which is capable of inspecting more than two sealed containers simultaneously. In that case, a same number of eddy-current displacement sensors to that of the containers which are accommodated in one chamber for inspection are disposed at predetermined position of the chamber, and these eddy-current displacement sensors are all controlled by a control device. In this case, although the number of containers which are inspected simultaneously is not particularly limited, it is preferably 10 to 100 from a view point of practical use and an industrial view point.