Process for the preparation of lithium intercalation compounds

(57) A summary and subject The conventional mixed oxide process for manufacturing the compound between lithium layers, It improves about a process parameter with important reaction time, reaction temperature, etc. , and the compound between lithium layers with good quality which was suitable as an activity substance in the electrode of the lithium secondary battery which is suitable as an activity substance in the electrode of a lithium secondary battery is manufactured cheaply. Solution means It is a production method of the compound between lithium layers by the heat solid phase reaction of the oxide of lithium hydroxide or lithium oxide, and a transition metal, or the mixture of an oxide catalyst precursor, a) It consists of each step of mixture in the aqueous suspension of the pulverizing powder of the above-mentioned ingredient in the 相応ing stoichiometry ratio, addition of b hydrogen peroxide, evaporation of c this reaction mixture and dryness of this powder, and the calcination 、 of d this powder.